Metal Distillation Separation Technology: The “Thermodynamic Code” for High Purity Metal Recycling

2025-04-01

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Under the wave of resource recycling and green manufacturing, metal 

recycling technology is becoming a core issue for sustainable industrial 

development. In the face of complex alloy waste, electronic waste and 

other high-value materials, traditional physical sorting and chemical 

leaching methods are often difficult to balance the efficiency and purity. 

With its unique thermodynamic principle, metal distillation separation 

technology has become the “invisible champion” for extracting 99.99% 

or more of high-purity metals from industrial waste. In this paper, the 

depth of the technology will be dismantled key processes and 

industrialization value.

Thermodynamic principle: boiling point 

difference-driven metal “purification”

The core of metal distillation is to utilize the boiling point difference of different 

metals in the alloy to achieve precise separation. Take zinc-lead alloy as an 

example, the boiling point of zinc (907℃) is significantly lower than that of lead 

(1749℃). When the liquid alloy is heated to the boiling temperature of zinc, 

the zinc is preferred to vaporize to form steam, while the lead remains liquid. 

Through a gradient condensation system, high boiling point impurities such 

as lead in the vapor are intercepted and liquefied at a specific temperature 

zone, and ultimately the high purity zinc vapor condensate is collected in a 

separate chamber.

The breakthrough of this technology is reflected 

in two major aspects:

Dynamic Temperature Control: Through multi-stage heating modules, the target 

metal vaporization temperature is precisely matched to avoid excessive energy 

consumption;

Multi-layer Condensation Barrier: Ceramic-based composite condenser tubes 

are used to reduce the temperature step-by-step in the vapor transmission 

path, which enhances the retention rate of the impurity metals to more than 98%.

Process innovation: from laboratory to industrial 

scale mass production

1. Evaporation system design

Vacuum environment optimization: distillation in 10-³Pa grade vacuum chamber, 

metal vaporization temperature is reduced by 30%-50%, energy consumption 

is saved by 40%;

Corrosion-resistant materials: evaporation crucible is coated with tungsten-molybdenum 

alloy, which is resistant to high temperature of 1600°C and acidic vapor corrosion, with

a life span of more than 5000 hours Continuous feeding mechanism: double locking

hopper sealing system realizes uninterrupted feeding of waste materials, and the

daily processing capacity of a single set of equipment can be up to 20 tons.

2. Condensation technology breakthrough

Directional condensation technology: extend the vapor path through the spiral deflector

plate, combined with the temperature difference in power generation and waste heat

recovery, condensation efficiency increased by 65%;

Contaminant interception network: multi-layer metal filter mesh aperture decreases

from 5mm to 0.1mm, and micron-sized particles are captured in stages.

3. Intelligent control system

online composition analysis: laser spectrometer real-time monitoring of vapor

composition, automatic adjustment of heating power and condensation temperature;

digital twin model: based on historical data to build a library of process parameters,

dynamic optimization of metal recovery rate and purity.

Application Scenario: Industrial Waste into 

High Purity Metal

1. Electronic Waste Regeneration

Recover gold, silver, palladium and other precious metals from waste circuit boards:

Gold recovery purity reaches 99.99%, and the output value of a single ton

of waste is increased by 80,000 yuan;

Copper-tin alloy separation efficiency exceeds 95%, and the acid leaching

wastewater discharge is reduced by 30%.

2. metallurgical slag treatment

zinc smelting fume extraction of indium, germanium and other strategic

metals, the recovery rate from 70% to 92%;

stainless steel slag separation of nickel, chromium, regeneration value of

each ton of slag over 5,000 yuan.

3. Aerospace materials regeneration

Titanium alloy waste is purified by distillation, and the oxygen content is

controlled below 200ppm to meet the standard of aviation forgings;

Cobalt and rhenium are recovered from high-temperature alloy waste, and

the purity is up to 4N level (99.99%), and the cost is only 1/3 of that of

mineral smelting.

Double breakthroughs in economic benefits and

environmental protection value

A recycled metal enterprise adopts metal distillation technology, and compared

with the traditional process, it achieves the following:

Cost Savings: tons of Cost savings: 55% reduction in energy consumption for

metal processing and 80% reduction in consumption of auxiliary materials;

Revenue growth: premium for high purity metal reaches 15%-30% of the average

market price, and annual revenue increases by 240 million yuan;

Environmental protection: heavy metal emission concentration is lower than

0.05mg/m³, and there is zero generation of dioxin, which has passed the

European Union's REACH certification.

It is estimated that the large-scale application of the technology can make

the world annually:

reduce 25 million tons of metal waste to landfill;

save 120 million tons of raw ore mining;

reduce carbon emissions by 8 million tons (equivalent to planting

460 million trees).

Technology Trend: From Single Separation to System Integration

Future metal distillation technology will evolve

in three major directions:

Multi-metal cogeneration system: a single distillation process to synchronously

separate more than three metals, such as copper-nickel-cobalt ternary alloy

purification in one step;

Microwave-assisted distillation: the introduction of microwave heating technology,

the speed of vaporization is increased by three times, suitable for nano-powder

recycling;

Modular mobile plant: the container-type distillation equipment can be deployed

directly in the Modularized mobile plant: containerized distillation equipment can be

deployed directly in mining areas or industrial parks, shortening the radius of

waste transportation.

Conclusion

Metal distillation and separation technology is rewriting the rules of the game in

resource recycling. It not only solves the problem of high-value utilization of

complex waste materials, but also realizes the precise closed loop of metal

recycling through “thermodynamic screening”. With the integration of intelligent

control, new materials and other technologies, this process will become an

indispensable “metal purification engine” in the green manufacturing system,

and promote industrial civilization to accelerate towards the goal of “zero waste”.